牛奶中的氯霉素分析
Chloramphenicol in Milk by LC-MS/MS
Conditions
Column: ACE 3 C18
Dimensions: 50 x 2.1 mm
Part Number: ACE-111-0502
Mobile Phase:
A: H2O
B: MeOH
Time(mins)
%B
0.00
10
0.05
10
2.50
95
3.00
95
3.10
10
4.50
10
Flow Rate: 0.5 mL/min
Injection: 10 μL
Detection: Bruker EVOQ Elite triple quad MS
VIP heated-ESI temperature: 400 °C
Cone gas temperature: 350 °C
Spray voltage: -4500 V